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Rev. Sci. Instrum. 82, 084102 (2011)

High-temperature and high-pressure pulsed synthesis apparatus for supercritical production of nanoparticles

Jakob R. Eltzholtz and Bo B. Iversen

The major limitation of continuous flow reactors is that the inherent distribution of residence times leads to broadening of the corresponding size distribution of the nanoparticles, and in addition it is not possible to carry out synthesis with very short or very long reaction times. Here a new synthesis concept is reported—pulsed synthesis—which removes the limitations of flow synthesis at the expense of a more complex reactor design and extensive computer control.

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